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Preparation of titanium dioxide nanotube arrays on titanium mesh by anodization in (NH4)(2)SO4/NH4F electrolyte
Zeng, Q-Y1,2; Xi, M.1; Xu, W.3; Li, X-J1
2013-11-01
Source PublicationMATERIALS AND CORROSION-WERKSTOFFE UND KORROSION
Volume64Issue:11Pages:1001-1006
AbstractThe self-organized titanium dioxide (TiO2) nanotube arrays on titanium mesh were prepared by electrochemical anodization with the neutral electrolyte containing ammonium sulfate and ammonium fluoride in a two-electrode electrochemical cell. The effects of the fluoride ion concentration, the anodic potential, and the oxidation time on the formation of the titanium dioxide nanostructures on titanium mesh with complex geometry were investigated. The anodized titanium mesh was characterized by field emission scanning electron microscope and in situ high temperature X-ray diffraction. The results show that the titanium dioxide nanotube arrays are grown in a radially outward direction around the titanium wire. The optimized anodization condition for preparing titanium dioxide nanotube arrays with superior architecture on the titanium mesh is 0.5wt% of ammonium fluoride, 20V of applied potential, and 20min of oxidation time. The amorphous titanium dioxide nanotubes on titanium mesh turn to anatase phase at 400 degrees C and further to rutile phase at 650 degrees C.
SubtypeArticle
KeywordAnodization Process Parameters Titanium Mesh Tio2 Nanotubes
WOS HeadingsScience & Technology ; Technology
DOI10.1002/maco.201106481
WOS Subject ExtendedMaterials Science ; Metallurgy & Metallurgical Engineering
WOS KeywordSENSITIZED SOLAR-CELLS ; TIO2 NANOTUBES ; OXIDE NANOTUBE ; ANODIC-OXIDATION ; ORGANIC ELECTROLYTE ; FABRICATION ; PHOTOANODES ; GROWTH ; TEMPERATURE ; ALLOY
Indexed BySCI
Language英语
WOS SubjectMaterials Science, Multidisciplinary ; Metallurgy & Metallurgical Engineering
WOS IDWOS:000328291000006
Citation statistics
Cited Times:14[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://ir.giec.ac.cn/handle/344007/10103
Collection中国科学院广州能源研究所
Affiliation1.Chinese Acad Sci, Guangzhou Inst Energy Convers, Key Lab Renewable Energy & Gas Hydrate, Guangzhou 510640, Guangdong, Peoples R China
2.Chinese Acad Sci, Grad Univ, Beijing 100049, Peoples R China
3.China Shipbldg Ind Corp, Environm Engn Co Ltd, Wuhan 430064, Peoples R China
Recommended Citation
GB/T 7714
Zeng, Q-Y,Xi, M.,Xu, W.,et al. Preparation of titanium dioxide nanotube arrays on titanium mesh by anodization in (NH4)(2)SO4/NH4F electrolyte[J]. MATERIALS AND CORROSION-WERKSTOFFE UND KORROSION,2013,64(11):1001-1006.
APA Zeng, Q-Y,Xi, M.,Xu, W.,&Li, X-J.(2013).Preparation of titanium dioxide nanotube arrays on titanium mesh by anodization in (NH4)(2)SO4/NH4F electrolyte.MATERIALS AND CORROSION-WERKSTOFFE UND KORROSION,64(11),1001-1006.
MLA Zeng, Q-Y,et al."Preparation of titanium dioxide nanotube arrays on titanium mesh by anodization in (NH4)(2)SO4/NH4F electrolyte".MATERIALS AND CORROSION-WERKSTOFFE UND KORROSION 64.11(2013):1001-1006.
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